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ChemInform Abstract: Synthesis and Characterization of New Potassium Pentafluoroantimonate(III) K2SbF5×1.5H2O.

✍ Scribed by L. A. ZEMNUKHOVA; V. YA. KAVUN; G. A. FEDORISHCHEVA; T. A. KAIDALOVA; R. L. DAVIDOVICH

Publisher
John Wiley and Sons
Year
2010
Weight
32 KB
Volume
29
Category
Article
ISSN
0931-7597

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✦ Synopsis

Synthesis and Characterization of New

-The title hydrate is synthesized by reaction of KNO 2 with SbF 3 (molar ratio 0.5:1 to 5:1) in water at room temperature. The new compound crystallizes in the rhombic system and appears to be isostructural to NaM 2 SbF 5 -type compounds. Spectral and thermal properties of the hydrate are studied.

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ChemInform Abstract: Synthesis, Thermal
ChemInform Abstract: Synthesis, Thermal Decomposition and Infrared Spectra of Two New Hydrazinium (1+) Fluorovanadates(III), (N2H5)2VF5×H2O and (N2H5)2VF5.
✍ A. RAHTEN; S. MILICEV 📂 Article 📅 2010 🏛 John Wiley and Sons ⚖ 37 KB 👁 2 views

3 . The IR spectra indicate the presence of N 2 H + 5 cations with different hydrogen bonding in all three hydrazinium compounds. The weak H bonds in these compounds are further weakened along the decomposition series. According to the powder XRD data, (I) consists of isolated [VF 5 •H 2 O] 2-octahe