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ChemInform Abstract: Syntheses of Novel Glycosylidene-spiro-heterocycles Related to Hydantocidin.

✍ Scribed by Erzsebet Osz; Laszlo Szilagyi; Laszlo Somsak; Attila Benyei

Publisher
John Wiley and Sons
Year
2010
Weight
33 KB
Volume
30
Category
Article
ISSN
0931-7597

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✦ Synopsis

Syntheses of Novel Glycosylidene-spiro-heterocycles Related to Hydantocidin. -Both anomers (III) and (IV), representing the first examples of glycosyl thiocyanates with a quaternary anomeric center, are prepared by reaction of bromide (I) with either KSCN or AgSCN. They are resistent to isomerization into isothiocyanates even at elevated temperatures and react with H 2 S under mild conditions to give the target spiro compounds.

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