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The crystal structure of monoclinic thallium(III) hydrogendiphosphate, TlHP 2 O 7 , has been solved from laboratory X-ray powder diffraction data and refined by the Rietveld method. All atoms occupy general positions. The Tl III ions have a distorted octahedral coordination environment of O atoms fr
## Abstract The crystal structure of Na~3~HP~2~O~7~ β H~2~O has been determined from X-ray powder diffraction data. The structure is monoclinic, space group __P__2~1~/__n__ (No. 14), with unit cell dimensions __a__ = 10.4242(1) Γ , __b__ = 6.8707(1) Γ , __c__ = 10.0837(1) Γ , __Ξ²__ = 99.2258(7)Β°, __V
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