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TlHP2O7: structure determination from X-ray powder diffraction data

✍ Scribed by Ivashkevich, Ludmila S. ;Selevich, Kirill A. ;Lyakhov, Alexander S. ;Selevich, Anatoly F.

Publisher
International Union of Crystallography
Year
2007
Tongue
English
Weight
308 KB
Volume
63
Category
Article
ISSN
1600-5368

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✦ Synopsis

The crystal structure of monoclinic thallium(III) hydrogendiphosphate, TlHP 2 O 7 , has been solved from laboratory X-ray powder diffraction data and refined by the Rietveld method. All atoms occupy general positions. The Tl III ions have a distorted octahedral coordination environment of O atoms from four diphosphate groups. Adjacent TlO 6 octahedra form edge-shared Tl 2 O 10 dimers which share corners with PO 4 tetrahedra to build a three-dimensional polymeric structure.

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