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ChemInform Abstract: Stable Endoperoxide of 4,5,6,8,16-Pentamethyl[2.2]metacyclophane; Structural Analysis and Deoxygenation.

✍ Scribed by T. SAWADA; K. MIMURA; T. THIEMANN; T. YAMATO; M. TASHIRO; S. MATAKA

Publisher: John Wiley and Sons
Year: 2010
Weight: 29 KB
Volume: 29
Category: Article
ISSN: 0931-7597
DOI: 10.1002/chin.199835143

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✦ Synopsis

Irradiation of metacyclophane (I) in different solvents such as acetone, ethanol, or hexane affords the endoperoxide (II) in high yields. The X-ray crystallographic analysis of (II) and its thermal deoxygenation reaction are described. -(SAWADA, T.;

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