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ChemInform Abstract: Solution-Phase Parallel Tetrahydrofuran Synthesis with Propargyl Alcohols and Benzylidene-(or Alkylidene-)malonates.

✍ Scribed by Marcello Cavicchioli; Xavier Marat; Nuno Monteiro; Benoit Hartmann; Genevieve Balme

Book ID
101930961
Publisher
John Wiley and Sons
Year
2010
Weight
29 KB
Volume
33
Category
Article
ISSN
0931-7597

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Solution-phase parallel tetrahydrofuran
Solution-phase parallel tetrahydrofuran synthesis with propargyl alcohols and benzylidene-(or alkylidene-)malonates
✍ Marcello Cavicchioli; Xavier Marat; Nuno Monteiro; Benoı̂t Hartmann; Geneviève B 📂 Article 📅 2002 🏛 Elsevier Science 🌐 French ⚖ 191 KB

A large array of 3-methylene tetrahydrofurans has been synthesized from propargylic alcohols and activated olefins. The reaction is promoted by copper iodide that is removed at the end of the reaction by simple filtration, affording the desired heterocycles in high yield and purity.