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ChemInform Abstract: Single-Stage Preparation of 2,4-Di(alkylthio)-3-methyl-1,3-imidazoles from Methyl Isothiocyanate.

โœ Scribed by L. BRANDSMA; N. A. NEDOLYA; H. D. VERKRUIJSSE; B. A. TROFIMOV


Publisher
John Wiley and Sons
Year
2010
Weight
28 KB
Volume
29
Category
Article
ISSN
0931-7597

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Synthesis of 2-methyl-4(5)-nitro[15N1(3)
โœ Jerzy Suwiล„ski; Wojciech Szczepankiewicz ๐Ÿ“‚ Article ๐Ÿ“… 1996 ๐Ÿ› John Wiley and Sons ๐ŸŒ French โš– 330 KB ๐Ÿ‘ 1 views

A simple four-stage conversion of 2-1nethyl-4(5>nitroimidazole to 2-methyl-4(5)-nitr0['~N""]imidazole is reported. The method consists in N-nitration of the initial compound to ?-methyl-1,4-dinitroimidazole, treating the latter with ["Nlglycine and N-dealkylation of the obtained (~-rnethyl-4-nitro[~