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ChemInform Abstract: Resolution of 2-Methylalkanoic Esters: Enantioselective Aminolysis by ( R)-1-Phenylethylamine of Ethyl 2-Methyloctanoate Catalyzed by Lipase B from Candida antarctica.

✍ Scribed by C. VOERDE; H.-E. HOEGBERG; E. HEDENSTROEM

Book ID
112038224
Publisher
John Wiley and Sons
Year
2010
Weight
30 KB
Volume
27
Category
Article
ISSN
0931-7597

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Resolution of 2-methylalkanoic esters: E
Resolution of 2-methylalkanoic esters: Enantioselective aminolysis by (R)-1-phenylethylamine of ethyl 2-methyloctanoate catalysed by lipase B from Candida antarctica
✍ Carin VΓΆrde; Hans-Erik HΓΆgberg; Erik HedenstrΓΆm πŸ“‚ Article πŸ“… 1996 πŸ› Elsevier Science 🌐 English βš– 448 KB

Enantiomerically pure (R)-l-phenylethylamine and ethyl rac-2methyloctanoate in the presence of lipase from Candidada antarctica (Novozym 435) reacted to give (R)-2-methyloctanoic (R)-l-phenylethylamide as the predominant diastereomer of 30 -40% de at = 100% conversion. Ethyl rac-2-methyldecanoate an