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ChemInform Abstract: Practical Synthesis of Amides from Alkynyl Bromides, Amines, and Water.

โœ Scribed by Zheng-Wang Chen; Huan-Feng Jiang; Xiao-Yan Pan; Zai-Jun He

Publisher
John Wiley and Sons
Year
2011
Weight
28 KB
Volume
42
Category
Article
ISSN
0931-7597

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Practical Synthesis of Unsymmetrical Polyamine Amides. -Careful monoacetylation of spermine (I) with ethyl trifluoroacetate followed by full N-protection and selective detrifluoroacetylation provides a one-pot procedure for the preparation of unsymmetrically protected polyamines (III). Their utilit