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ChemInform Abstract: Oxidation of Azines. Part 2. Synthesis and Molecular Structure of 3,4- Dihydroxy-1-methyl-2-oxo-4-(γ-pyridyl)piperidine.

✍ Scribed by I. A. BEKRO; A. T. SOLDATENKOV; A. I. STASH; N. YU. CHERNIKOVA; A. I. CHERNYSHEV

Publisher
John Wiley and Sons
Year
2010
Weight
30 KB
Volume
28
Category
Article
ISSN
0931-7597

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✦ Synopsis

Abstract

ChemInform is a weekly Abstracting Service, delivering concise information at a glance that was extracted from about 100 leading journals. To access a ChemInform Abstract of an article which was published elsewhere, please select a “Full Text” option. The original article is trackable via the “References” option.

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Two isomeric pairs of compounds, cis-and trans-2morpholino-2-thiono-4-methyl-1,3,2-dioxaphosphinane (1A ‫ם‬ 1B) and 2-morpholino-2-oxo-4-methyl-1,3,2-dioxaphosphinane (2A ‫ם‬ 2B) were obtained and separated into the pure compounds by silica gel chromatography. Attempts at crystallization afforded 1A