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ChemInform Abstract: New Synthesis of t-Butyl Arylpropiolates Using Diazo(trimethylsilyl)methylmagnesium Bromide.

✍ Scribed by Yoshiyuki Hari; Koji Date; Ryosuke Kondo; Toyohiko Aoyama

Publisher: John Wiley and Sons
Year: 2008
Weight: 28 KB
Volume: 39
Category: Article
ISSN: 0931-7597
DOI: 10.1002/chin.200845095

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The Improved Synthesis of β-D-Glucuronides Using TEMPO and t-Butyl Hypochlorite. -β-D-Glucuronides (II) as well as 13 C-labeled derivatives are prepared, using oxidation of the corresponding glucosides (I) by t-butyl hypochlorite and tetramethylpiperidinyl-1-oxyl as the key step.