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ChemInform Abstract: The Improved Synthesis of β-D-Glucuronides Using TEMPO and t-Butyl Hypochlorite.

✍ Scribed by Fiona Melvin; Alan McNeill; Peter J. F. Henderson; Richard B. Herbert

Publisher: John Wiley and Sons
Year: 2010
Weight: 33 KB
Volume: 30
Category: Article
ISSN: 0931-7597
DOI: 10.1002/chin.199921204

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✦ Synopsis

The Improved Synthesis of β-D-Glucuronides Using TEMPO and t-Butyl Hypochlorite.

-β-D-Glucuronides (II) as well as 13 C-labeled derivatives are prepared, using oxidation of the corresponding glucosides (I) by t-butyl hypochlorite and tetramethylpiperidinyl-1-oxyl as the key step.

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