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ChemInform Abstract: Microwave Irradiation — An Important Tool to Functionalize Fullerenes and Carbon Nanotubes

✍ Scribed by Fernando Langa; Pilar de la Cruz

Publisher
John Wiley and Sons
Year
2008
Weight
15 KB
Volume
39
Category
Article
ISSN
0931-7597

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ChemInform Abstract: New Route to Functionalized Cyclohexenes from Nitromethane and Electrophilic Alkenes Without Solvent under Focused Microwave Irradiation.
✍ D. MICHAUD; S. ABDALLAH-EL AYOUBI; M.-J. DOZIAS; L. TOUPET; F. TEXIER-BOULLET; J 📂 Article 📅 2010 🏛 John Wiley and Sons ⚖ 31 KB

The title reaction affords two isomers of new cyclohexenes like (III) via a diastereoselective double Michael addition in the presence of a catalytic amount of piperidine. A stoichiometric amount of piperidine promotes the demethoxycarbonylation of compounds (III) to hexenes such as (IV). -