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ChemInform Abstract: Improved Synthesis of Phenylacetamides by the Willgerodt Reaction with Microwave Heating.

✍ Scribed by C. R. STRAUSS; R. W. TRAINOR

Book ID
112024384
Publisher
John Wiley and Sons
Year
2010
Weight
27 KB
Volume
26
Category
Article
ISSN
0931-7597

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The Willgerodt-Kindier reaction of several awl aikyl ketones with sulfur and morpholine under solvent-free conditions was performed in a domestic microwave oven. Good yields were attained within a very short reaction time (between 3.5-6 rain.).