The rapid synthesis of thiomorpholides by Willgerodt-Kindler reaction under microwave heating

✍ Scribed by Masoud Nooshabadi; Kioumars Aghapoor; Hossein Reza Darabi; Mohammad Majid Mojtahedi

• Book ID: 104262378
• Publisher: Elsevier Science
• Year: 1999
• Tongue: French
• Weight: 159 KB
• Volume: 40
• Category: Article
• ISSN: 0040-4039
• DOI: 10.1016/s0040-4039(99)01600-7

✦ Synopsis

The Willgerodt-Kindier reaction of several awl aikyl ketones with sulfur and morpholine under solvent-free conditions was performed in a domestic microwave oven. Good yields were attained within a very short reaction time (between 3.5-6 rain.).