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ChemInform Abstract: Identification of the S-4 Radical Anion in Solution.

✍ Scribed by E. LEVILLAIN; P. LEGHIE; N. GOBELTZ; J. P. LELIEUR

Publisher
John Wiley and Sons
Year
2010
Weight
27 KB
Volume
28
Category
Article
ISSN
0931-7597

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200 mL) was acidified with 3 drops of 32% HCI and stirred for 15 min at 50Β°C (exclusion of light). After extraction with CH,CI,, the organic phase was dried (Na,SO,) and purified on silica gel (20 8). After removal of the solvent there remained 0.53 g (72%) of a crystalline product. For further puri