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ChemInform Abstract: Facile Synthesis of (+)- and (-)-Geissman-Waiss Lactones.

✍ Scribed by T. KOUYAMA; H. MATSUNAGA; T. ISHIZUKA; T. KUNIEDA

Publisher
John Wiley and Sons
Year
2010
Weight
27 KB
Volume
28
Category
Article
ISSN
0931-7597

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Synthesis of (R)-and (S)-3-(tert-Butyldimethylsilyloxy)-1-pyrroline N-Oxides -Chiral Nitrones for Synthesis of Biologically Active Pyrrolidine Derivative, Geissman-Waiss Lactone. -Tungstatemediated oxidation of the chiral Tbs-protected 3-hydroxypyrrolidines (II) provides the required nitrones (III)