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ChemInform Abstract: Efficient Synthesis of Primary 2-Aminothiols from 2-Aminoalcohols and Methyldithioacetate.

✍ Scribed by Guillaume Mercey; Delphine Bregeon; Annie-Claude Gaumont; Jocelyne Levillain; Mihaela Gulea

Publisher: John Wiley and Sons
Year: 2009
Weight: 51 KB
Volume: 40
Category: Article
ISSN: 0931-7597
DOI: 10.1002/chin.200909199

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## Abstract magnified image Condensation of aminoalcohols with 2‐HC(O)C~6~H~4~B(OH)~2~ afforded the macrocyclic compounds 1–7 with an OBOBO structural unit. Crystals of **1** were triclinic, space group P‐1, a = 9.9818(12) Å, b = 12.8302(15) Å, c = 13.1663(15) Å, α = 105.503(2)°, β = 94.860(2)°, γ

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