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ChemInform Abstract: Dihydroxylation of 4-Substituted 1,2-Dioxines: A Concise Route to Branched Erythro Sugars.

โœ Scribed by Tony V. Robinson; Daniel Sejer Petersen; Dennis K. Taylor; Edward R. T. Tiekink

Publisher
John Wiley and Sons
Year
2009
Weight
59 KB
Volume
40
Category
Article
ISSN
0931-7597

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Reaction of 2,2,6-Trimethyl-4H-1,3-dioxin-4-one with Imines: An Easy Route to Enamides. -Thermolysis of the dioxin (I) generates an acylketene which is readily trapped by imines to give the N-alkenyl acetoacetamides (III). They are useful intermediates in oxidative radical cyclizations leading to .