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ChemInform Abstract: Copper-Catalyzed Cross-Coupling of α-Seleno-acylzirconocene Chloride with Haloalkynes: Synthesis of α-Seleno-Substituted Vinyl Alkynyl Ketones.

✍ Scribed by Ai-Ming Sun; Xian Huang

Publisher: John Wiley and Sons
Year: 2010
Weight: 31 KB
Volume: 31
Category: Article
ISSN: 0931-7597
DOI: 10.1002/chin.200026173

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The copper-catalyzed cross-coupling reaction of ␣-selenoacylzirconocene chloride 3 with haloalkynes in the presence of carbon monoxide gives ␣seleno-substituted vinyl alkynyl ketones 5 in moderate yields. The reaction conditions are neutral and mild enough (room temperature, 1 atm carbon monoxide) t

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