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ChemInform Abstract: Conjugate Addition of Organocuprates to Diethyl Vinylphosphonate.

โœ Scribed by I. C. BALDWIN; R. P. BECKETT; J. M. J. WILLIAMS

Book ID
112033360
Publisher
John Wiley and Sons
Year
2010
Weight
28 KB
Volume
27
Category
Article
ISSN
0931-7597

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Synthesis of 3-Oxoalkylphosphonates via the Conjugate Addition of Acylcuprates to Diethyl Vinylphosphonate. -Acylcuprates, generated in situ from dialkylcyanocuprates (I) and carbon monoxide, are added to vinylphosphonate (III) to give, after hydrolysis, phosphonates (IV) in good yields. Phosphonat