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ChemInform Abstract: Axinellamines A and B, New Pyrrole Alkaloids of the Marine Sponge Axinella sp.

โœ Scribed by K. C. BASCOMBE; S. R. PETER; W. F. TINTO; S. M. BISSADA; S. MCLEAN; W. F. REYNOLDS

Publisher
John Wiley and Sons
Year
2010
Weight
26 KB
Volume
29
Category
Article
ISSN
0931-7597

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Scheme 2. Synthesis of the achiral building block 7; reagents: (a) ICH 2 CO 2 Et, FeSO 4 โ€ข7H 2 O, H 2 O 2 , DMSO (72%); (b) (Boc) 2 O, DMAP, MeCN (93%); (c) DIBAL, CH 2 Cl 2 ; (d) (EtO) 2 P(O)CH 2 -CO 2 Et, NaH, THF (63% based on 3); (e) MnO 2 , CHCl 3 Scheme 3. Synthesis of (S)-axinellamine A (1);