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ChemInform Abstract: Asymmetric Deprotonation of N,N-Dihexyl-1-naphthamides to Provide Atropisomers of N,N-Dihexyl-2-alkyl-1-naphthamides.

✍ Scribed by S. THAYUMANAVAN; P. BEAK; D. P. CURRAN

Book ID: 112035860
Publisher: John Wiley and Sons
Year: 2010
Weight: 27 KB
Volume: 27
Category: Article
ISSN: 0931-7597
DOI: 10.1002/chin.199633030

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Atroposelective olefination of axially chiral N,N-dialkyl 2-formyl-1-naphthamides with chiral ligand-derived stable arsonium ylides proceeded in a kinetic resolution manner. The (E)-olefin products were obtained in excellent chemical yields and in up to 88:12 diastereoselectivity. Effects of the ami