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ChemInform Abstract: An Improved, Large-Scale (90 g) Synthesis of Bis(tetraethylammonium)bis(1,3-dithiole-2-thione-4,5-dithiol)zincate: Synthesis and X-Ray Crystal Structures of Bicyclic and Tricyclic 1,4-Dithiocines Derived from 1,3-Dithiole-2-thione-4,5-dithiolate (DMIT).

✍ Scribed by C. WANG; A. S. BATSANOV; M. R. BRYCE; J. A. K. HOWARD


Publisher
John Wiley and Sons
Year
2010
Weight
33 KB
Volume
30
Category
Article
ISSN
0931-7597

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Synthesis and Crystal Structures of Bis(
✍ Harald MΓΌller; Anna Puig Molina; B. Zh. Narymbetov; L. V. Zorina; S. S. Khasanov πŸ“‚ Article πŸ“… 1998 πŸ› John Wiley and Sons 🌐 German βš– 112 KB πŸ‘ 1 views

The title compounds were prepared from 1,3,4,6tetrathiapentalene-2,5-dione (1) in one step via the in situ The X-ray single crystal structure of (Et 4 N) 2 [Zn(dmid) 2 ] (3 a) gave the tetragonal space group P4 3 2 1 2 with a = b = 13.810(2) A Ê , c = 16.480(3) A Ê , and Z = 4. (n-Bu 4 N) 2 [Zn(dmi