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ChemInform Abstract: An Enantioselective Synthesis of (-)-Allosamidin by Asymmetric Desymmetrization of a Highly Functionalized meso-Epoxide.

✍ Scribed by Darren J. Kassab; Bruce Ganem

Publisher
John Wiley and Sons
Year
2010
Weight
34 KB
Volume
30
Category
Article
ISSN
0931-7597

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✦ Synopsis

An Enantioselective Synthesis of (-)-Allosamidin by Asymmetric Desymmetrization of a Highly Functionalized meso-Epoxide.

-The enantioselective preparation of (XII) represents a formal total synthesis of (-)-allosamidin (XIII). A significant improvement compared to prior approaches affords this intermediate (XII) in only 9 steps from the cyclopentene (I) with 25% overall yield and 94% e.e. -(KASSAB,

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