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ChemInform Abstract: A Simple and Convenient Synthetic Method for α-Trifluoromethylpyridines.

✍ Scribed by E. OKADA; T. KINOMURA; Y. HIGASHIYAMA; H. TAKEUCHI; M. HOJO

Publisher
John Wiley and Sons
Year
2010
Weight
33 KB
Volume
29
Category
Article
ISSN
0931-7597

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Reaction of α,β-unsaturated trifluoromethyl ketones (I) with primary enamines in the presence of POCl 3 and pyridine adsorbed on silica gel and following oxidation of the resulting dihydropyridines provides a high-yielding synthesis of title compounds (III) (16 examples). -(KATSUYAMA, I.; OGAWA,