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ChemInform Abstract: A Prototypical Reagent for the Synthesis of Substituted Hydrazines.

✍ Scribed by U. MAEEORG; L. GREHN; U. RAGNARSSON

Publisher
John Wiley and Sons
Year
2010
Weight
27 KB
Volume
28
Category
Article
ISSN
0931-7597

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Prototypical Reagent for the Synthesis o
Prototypical Reagent for the Synthesis of Substituted Hydrazines
✍ Dr. Uno MΓ€eorg; Dr. Leif Grehn; Dr. Ulf Ragnarsson πŸ“‚ Article πŸ“… 1996 πŸ› John Wiley and Sons 🌐 English βš– 484 KB πŸ‘ 1 views

gelatin \* solids yield. 'H NMR (270 MHz. CDCI,): b =1.42 (s, 18H. NBoc,), 1.49 (s, 9H. NHBoc), 5.26 (5, 2H, CH,Ph), 7. 30-7.41 (brm, 5 H, Ph). Compound 3, dissolved in CH,OH (500 mL). was hydrogenolyzed over PdjC (S%/carbon. 1.2 g) for 3 h. When TLC indicated complete reaction, the catalyst was fil