ChemInform Abstract: A Practical Reagent for the Synthesis of Substituted Hydrazines.
β Scribed by L. GREHN; B. NYASSE; U. RAGNARSSON
- Publisher
- John Wiley and Sons
- Year
- 2010
- Weight
- 28 KB
- Volume
- 29
- Category
- Article
- ISSN
- 0931-7597
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gelatin \* solids yield. 'H NMR (270 MHz. CDCI,): b =1.42 (s, 18H. NBoc,), 1.49 (s, 9H. NHBoc), 5.26 (5, 2H, CH,Ph), 7. 30-7.41 (brm, 5 H, Ph). Compound 3, dissolved in CH,OH (500 mL). was hydrogenolyzed over PdjC (S%/carbon. 1.2 g) for 3 h. When TLC indicated complete reaction, the catalyst was fil
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