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ChemInform Abstract: A Practical Synthesis of the First P-Phosphinoylmethyl-λ5-phosphazenes.

✍ Scribed by M. Alajarin; C. Lopez-Leonardo; P. Llamas-Lorente; D. Bautista


Publisher
John Wiley and Sons
Year
2001
Weight
33 KB
Volume
32
Category
Article
ISSN
0931-7597

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ChemInform Abstract: A Practical Synthes
✍ Erick R. R. Young; Raymond L. Funk 📂 Article 📅 2010 🏛 John Wiley and Sons ⚖ 27 KB 👁 1 views

The practical multigram synthesis of the title compound (IV) involves a crucial intramolecular acyloin condensation of the diester with excess sodium in refluxing THF. The dione (IV) is obtained in high yield after aerobic work-up. -(YOUNG, ERICK