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ChemInform Abstract: A Convenient Two-Step One-Pot Synthesis of Phosphonamidates.

✍ Scribed by K. L. MLODNOSKY; H. M. HOLMES; V. Q. LAM; C. E. BERKMAN

Publisher: John Wiley and Sons
Year: 2010
Weight: 28 KB
Volume: 29
Category: Article
ISSN: 0931-7597
DOI: 10.1002/chin.199811222

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✦ Synopsis

A Convenient Two-Step One-Pot Synthesis of Phosphonamidates.

-Phosphoramidates (IV) of glutamic acid, potential inhibitors of glutamyl hydrolases, are prepared by 1H-tetrazole catalyzed reaction of phosphonyl dichloride (I) with alcohols and glutamic acid benzyl ester. Undesired disubstitution of (I) by the alcohols is minimized due to the presence of 1H-tetrazole.

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