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ChemInform Abstract: ((3-Dimethylamino)propyl)dimethylaluminum: A Convenient Reagent for Methylation and Ethynylation of Carbonyl Compounds.

✍ Scribed by W. BAIDOSSI; A. ROSENFELD; B. C. WASSERMANN; S. SCHUTTE; H. SCHUMANN; J. BLUM

Publisher
John Wiley and Sons
Year
2010
Weight
34 KB
Volume
28
Category
Article
ISSN
0931-7597

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✦ Synopsis

The title reagent (I) methylates a variety of mono-and diketones such as (II), (IV), (VII), or (IX). Aromatic aldehydes (XI) and (XIII) undergo simple methylation only after activation with AlCl3. Reaction of (I) with terminal acetylenes (XVI) allows the carbonyl-alkynylation of diphenyl ketone (IIa). -(BAIDOSSI, W.;

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