3-Chloropropyl phenyl ether as a 1,3-dil
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Francisco Foubelo; Miguel Yus
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Article
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1999
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Elsevier Science
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French
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The reaction of 3-chloropropyl phenyl ether (1) with lithium powder and a catalytic amount of DTBB (2.5% molar) in THF at -78ยฐC followed by successive treatment with a carbonyl compound [El = ButCHO, Me2CO, (CH2)5CO] at -78 to 20ยฐC and, after 1 h at this temperature, a second one [F~ = ButCHO, PhCHO