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Chemical synthesis of15N-labeled analogues of zervamicin IIB

✍ Scribed by W. H. Rimawi; An. A. Ogrel; J. Raap; V. I. Shvets

Book ID
110669751
Publisher
SP MAIK Nauka/Interperiodica
Year
2000
Tongue
English
Weight
773 KB
Volume
26
Category
Article
ISSN
1068-1620

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For the first time the total synthesis of the peptaibol zervamicin IIB is described. Synthesis of this peptaibol was achieved by the Fmoc/tert-butyl strategy in solution using a fragment condensation approach. Three fragments of zervamicin IIB were obtained by stepwise elongation with Fmoc amino aci

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## Abstract Zervamicin IIB is a member of the α‐aminoisobutyric acid containing peptaibol antibiotics. A new procedure for the biosynthetic preparation of the uniformly ^13^C‐ and ^15^N‐enriched peptaibol is described. This compound was isolated from the biomass of the fungus‐producer __Emericellop