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Chemical and Thermodynamic Properties of Methyl Chloride Dimer Radical Cations in the Gas Phase

✍ Scribed by de Visser, Sam P.; de Koning, Leo J.; Nibbering, Nico M. M.


Book ID
126894490
Publisher
American Chemical Society
Year
1998
Tongue
English
Weight
140 KB
Volume
120
Category
Article
ISSN
0002-7863

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200 mL) was acidified with 3 drops of 32% HCI and stirred for 15 min at 50Β°C (exclusion of light). After extraction with CH,CI,, the organic phase was dried (Na,SO,) and purified on silica gel (20 8). After removal of the solvent there remained 0.53 g (72%) of a crystalline product. For further puri