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Charge-State-Dependent Sequence Analysis of Protonated Ubiquitin Ions via Ion Trap Tandem Mass Spectrometry

โœ Scribed by Reid, Gavin E.; Wu, Jin; Chrisman, Paul A.; Wells, J. Mitchell; McLuckey, Scott A.

Book ID
126406381
Publisher
American Chemical Society
Year
2001
Tongue
English
Weight
251 KB
Volume
73
Category
Article
ISSN
0003-2700

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## Abstract Two heptapeptides have been prepared by Fmoc methodology using Wang resin as solid support. For attachment of the first amino acid, several coupling systems were evaluated, and DIC/DMAP system could give yields of >99% and low levels of racemization. The selection of scavenger combinati