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Characterization of tetraene intermediates formed in the [3+2]-photocycloaddition of 1,4-dicyano-6-methylnaphthalene with styrene

โœ Scribed by Hideo Shiratori, Yuki Nogami, Yasuo Kubo

Book ID
118809746
Publisher
Springer Netherlands
Year
2012
Tongue
English
Weight
758 KB
Volume
39
Category
Article
ISSN
0922-6168

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Ethylcrotonates in the Synthesis of 4,4-Disubstituted 3,5-Dicyano-6oxo-1,4,5,6-tetrahydropyridine-2-thiolates. -Michael addition of ethyl crotonate (I) to cyanothioacetamide (II) in the presence of N-methylmorpholine and subsequent in situ cyclization affords the title tetrahydropyridinethiolates as