✦ LIBER ✦

Characterization and determination of PCB isomers by high resolution gas chromatography and HRGC/mass spectrometry

✍ Scribed by Onuska, F. I. ;Terry, K. A.

Publisher: John Wiley and Sons
Year: 1986
Tongue: English
Weight: 366 KB
Volume: 9
Category: Article
ISSN: 0935-6304
DOI: 10.1002/jhrc.1240091116

No coin nor oath required. For personal study only.

✦ Synopsis

An integrated analytical procedure for polychlorinated biphenyl (PCB) multiresidues in environmental samples has been developed and applied to well-characterized samples. PCB residues are characterized and quantified using wall coated open tubular column (WCOT) gas chromatography or HRGC/MS-selected ion monitoring. An automated data system based on a Spectra Physics SP-4200 computing integrator is used to select and quantitate peaks of individual congeners and homolog groups. This procedure consistently yields results with a reproducibility within 3 percent for HRGC-ECD and 3.7 percent for HRGC/MS-SIM technique respectively.

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