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Cellulose organic solvents. I. The structures of anhydrous N-methylmorpholine N-oxide and N-methylmorpholine N-oxide monohydrate

✍ Scribed by Maia, E. ;Peguy, A. ;Pérez, S.

Book ID
114527959
Publisher
International Union of Crystallography
Year
1981
Weight
515 KB
Volume
37
Category
Article
ISSN
0567-7408

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Synthesis of N-methylmorpholine N-(17O-o
Synthesis of N-methylmorpholine N-(17O-oxide) and N-methylmorpholine 15N-(17O-oxide)
✍ Martina Opietnik; Antje Potthast; Takuya Kitaoka; Thomas Rosenau 📂 Article 📅 2009 🏛 John Wiley and Sons 🌐 French ⚖ 95 KB 👁 1 views

## Abstract __N__‐Methylmorpholine __N__‐(^17^O‐oxide) and __N__‐methylmorpholine __^15^N__‐(^17^O‐oxide) were prepared from __N__‐methylmorpholine and __^15^N__‐methylmorpholine by oxidation with H~2~ ^17^O~2~. The facile one‐pot procedure provided yields of 82 and 76%, respectively. The labeled h