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Cathodic alkylation of (methyl phenylacetate)tricarbonylchromium

โœ Scribed by A. A. Vasil'ev; V. A. Petrosyan

Book ID
112448586
Publisher
Springer
Year
1991
Tongue
English
Weight
55 KB
Volume
40
Category
Article
ISSN
1573-9171

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โœ Fujie Tanaka; Kaoru Fuji ๐Ÿ“‚ Article ๐Ÿ“… 1992 ๐Ÿ› Elsevier Science ๐ŸŒ French โš– 238 KB

Deprotonation of methyl phenylacetate with lithium diisopropylamide in tetrahydrofuran followed by trapping with trimethylsilyl chloride afforded an 81:19 mixture of E-and Z-silyl ketene acetals in agreement with a prediction by the calculation by Dauben. The E-silyl ketene acetal was readily isomet