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catena-Poly[[tetra­aqua­manganese(II)]-μ-6,6′-dihydr­oxy-3,3-diazenediyldibenzoato-κ2O:O′]

✍ Scribed by Tang, Yun-Zhi ;Tan, Yu-Hui ;Cao, Yan-Wen

Publisher
International Union of Crystallography
Year
2007
Tongue
English
Weight
120 KB
Volume
63
Category
Article
ISSN
1600-5368

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In the title compound, [Mn(C 14 H 8 N 2 O 6 )(H 2 O) 4 ] n , each 6,6 0dihydroxy-3,3 0 -diazenediyldibenzoate ligand acts as a carboxylate bridge, leading to the formation of polymeric chains running in the [110] direction. The Mn atom is hexacoordinated in a distorted octahedral geometry by six O a

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Single-crystal X-ray study T = 213 K Mean '(C±C) = 0.005 A Ê R factor = 0.030 wR factor = 0.086 Data-to-parameter ratio = 12.2 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.

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In the crystal structure of the polymeric title compound, [Mn(C~10~H~8~N~2~)(C~10~H~8~O~5~)(H~2~O)]~__n__~, the Mn^II^ atom is __O__,__O__′-chelated by the aromatic carboxylate end of the 3-(4-carboxylatophenoxy)propionate dianion and is covalently bonded (through one O atom) by the aliphatic carbox

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Single-crystal X-ray study T = 298 K Mean '(C±C) = 0.007 A Ê R factor = 0.054 wR factor = 0.131 Data-to-parameter ratio = 15.2 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.