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Catalytic Synthesis of Heterocycles. IX. 1 Dehydrocyclization of 2-Methyl-5-ethyl-4-pyridinethiol to 6-Methyl-5-azathianaphthene

โœ Scribed by HANSCH, CORWIN; CARPENTER, WAYNE

Book ID
127075236
Publisher
American Chemical Society
Year
1957
Tongue
English
Weight
508 KB
Volume
22
Category
Article
ISSN
0022-3263

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Synthesis of ethyl 5-cyano-6-hydroxy-2-methyl-4-(1-naphthyl)-nicotinate
โœ Yongchang Zhou; Tatsuro Kijima; Shunsuke Kuwahara; Masataka Watanabe; Taeko Izum ๐Ÿ“‚ Article ๐Ÿ“… 2008 ๐Ÿ› Elsevier Science ๐ŸŒ French โš– 174 KB

A novel ethyl 5-cyano-6-hydroxy-2-methyl-4-(1-naphthyl)-nicotinate is successfully synthesized and the structure is determined by XRD, GC-MS analysis, element analysis and NMR spectroscopic in detail. A reaction mechanism for the reaction is proposed.