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Catalytic Hydrogenation. II. A New, Convenient Technique for Laboratory Hydrogenations. A Simple, Automatic Device for Atmospheric Pressure Hydrogenations

✍ Scribed by Brown, Charles A.; Brown, Herbert C.


Book ID
120161514
Publisher
American Chemical Society
Year
1966
Tongue
English
Weight
927 KB
Volume
31
Category
Article
ISSN
0022-3263

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A simple apparatus is described for the generation of isotopic hydrogen gas by acid-catalysed hydrolysis of sodium borotritide or borodeuteride. The apparatus may be conveniently utilised for isotopic hydrogen reductions of from 20 urn01 to 1 mmol scale.