This book provides both an introduction for the novice and a review for the expert to the rapidly developing field of 13 C NMR spectroscopy of biological systems. It consists of a forward by Joachim Seelig, a preface by the author, and six chapters dealing with basic principles and key applications.
Carbon-13 NMR study of isoxazolopyridine systems
✍ Scribed by Stefano Chimichi; Piero Tedeschi; Alfredo Camparini; Fabio Ponticelli
- Publisher
- John Wiley and Sons
- Year
- 1982
- Tongue
- English
- Weight
- 285 KB
- Volume
- 20
- Category
- Article
- ISSN
- 0749-1581
No coin nor oath required. For personal study only.
✦ Synopsis
Abstract
The ^13^C NMR spectra of all azabenzenoid isoxazolopyridines and some of their chloro derivatives are discussed. All ^13^C resonances were unambiguously assigned by means of gated decoupled spectra, from which one‐bond and long‐range ^13^C^1^H coupling constants have been determined from line splittings.
📜 SIMILAR VOLUMES
13CNMR chemical shifts of 23 aniline and 1.8diaminonaphthalene derivatives are reported; the parent compounds are also included for purposes of comparison.
The 13C NMR spectra of thiazolopyridine systems are discussed. One-bond and long-range 13C-1H coupling constants were determined from line splittings and a simple method for distinguishing between 2-methylthiazoloand 3-methylisothiazolopyridines is suggested.
The =C NMR spectra of oxazolopyridine systems are discussed, and a simple method for distinguishing between 2-methyloxazolo- and3-metbylisoxazolo-pyridines is suggested, b e d on the & m i d shift of the methyl group. The effect of the 2-methyloxazole fusion on the pyridine ring is comparable to tha
## Abstract All four fully aromatic isothiazolopyridine isomers have been synthesized, their ^13^C spectra have been assigned and all one‐bond and long‐range ^13^C^1^H coupling constants have been determined.
## Abstract The carbon‐13 NMR spectra of a series of __exo__‐and __endo__‐epimers of 2‐substituted benzonorbornene (2‐substituent = OH, OCHO, Br, NH~2~, NHMe or NMe~2~) have been examined. The spectra are readily assigned by comparison with the coupled and off‐resonance proton decoupled spectra as