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(C24H20P)2[Mo6Cl14]

✍ Scribed by White, M. A. ;Pressprich, M. R. ;Coppens, P.

Book ID: 114510880
Publisher: International Union of Crystallography
Year: 1994
Tongue: English
Weight: 306 KB
Volume: 50
Category: Article
ISSN: 0108-2701
DOI: 10.1107/s0108270193013149

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NH 4 ) 2 [Mo 6 Cl 14 ] ´H2 O (1) was prepared from reactions of MoCl 2 in ethanol with aqueous NH 4 Cl solution. It crystallizes in the monoclinic space group I2/a (no. 15), Z = 4 with a = 912.3(1), b = 1491.2(2), c = 1724.8(2) pm, b = 92.25(1)°; R1 = 0.023 (based on F values) and wR2 = 0.059 (based