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Bromination of Cyclohexa-1,3-diene and ( R , S )-Cyclohexa-3,5-diene-1,2-diol

✍ Scribed by Han, Xinghua; Khedekar, Rajashree N.; Masnovi, John; Baker, Ronald J.

Book ID: 126453388
Publisher: American Chemical Society
Year: 1999
Tongue: English
Weight: 127 KB
Volume: 64
Category: Article
ISSN: 0022-3263
DOI: 10.1021/jo990473s

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## Abstract Polymerization of cyclohexa‐1,3‐diene using __sec__‐BuLi as initiator in cyclohexane produces both soluble (70–90 wt.‐%) and insoluble (10–30 wt.‐%) fractions depending on the temperature. The insoluble poly(cyclohexa‐1,3‐diene) was crystalline as determined by X‐ray diffraction and dif