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Blue Phosphors of Dinuclear and Mononuclear Copper(I) and Silver(I) Complexes of 3,5-Bis(trifluoromethyl)pyrazolate and the Related Bis(pyrazolyl)borate

โœ Scribed by Omary, Mohammad A.; Rawashdeh-Omary, Manal A.; Diyabalanage, Himashinie V. K.; Dias, H. V. Rasika

Book ID
120491514
Publisher
American Chemical Society
Year
2003
Tongue
English
Weight
65 KB
Volume
42
Category
Article
ISSN
0020-1669

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An improved synthesis of 3,5-bis(trifluoromethyl)pyrazole (1) is described. This compound was used for the high-yield syntheses of the tris(pyrazoly1)borates Nd [HB(3,,-pz),1 (2a) and the corresponding potassium salt, 2b, starting from 1 and NaBH, and KBH,, respectively. A convenient route to the co