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Bis(tert-butyl isocyanide)hexadecacarbonylhexaosmium

✍ Scribed by Orpen, A. G. ;Sheldrick, G. M.

Book ID
114525734
Publisher
International Union of Crystallography
Year
1978
Weight
338 KB
Volume
34
Category
Article
ISSN
0567-7408

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The title compound, [Mo(C 5 H 9 N) 3 (CO) 3 ], was produced from Mo(CO) 6 and tert-butyl isocyanide in the presence of 10 atm of carbon monoxide (1 atm = 101325 Pa). The octahedral complex shows a facial arrangement of the ligands, the Mo-C distances of the isocyanide ligands being about 0.15 A ˚lon