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Bis[N,N′-bis­(octylsulfanyl)glyoximato]nickel(II)

✍ Scribed by Gurol, Ilke ;Gumus, Gulay ;Yuksel, Fatma ;Jeanneau, Erwann ;Ahsen, Vefa

Book ID
104488655
Publisher
International Union of Crystallography
Year
2006
Tongue
English
Weight
232 KB
Volume
62
Category
Article
ISSN
1600-5368

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✦ Synopsis

In the title compound, [Ni(C 18 H 35 N 2 O 2 S 2 ) 2 ], the coordination geometry around the Ni atom, lying on a centre of symmetry, is square planar, consisting of four N atoms from the two vicdioxime ligands. The O atoms are intramolecularly hydrogen bonded, as is usually observed for anti-isomer metal complexes of vic-dioximes.

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Redetermination of bis­(di­methyl­glyoximato-κ2N,N′)­nickel(II)
✍ Li, Dai-Xi ;Xu, Duan-Jun ;Xu, Yuan-Zhi 📂 Article 📅 2003 🏛 International Union of Crystallography 🌐 English ⚖ 280 KB

Single-crystal X-ray study T = 295 K Mean '(C±C) = 0.005 A Ê R factor = 0.034 wR factor = 0.103 Data-to-parameter ratio = 13.3 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.