Copper diacetate monohydrate (0.20 g, 1 mmol) was dissolved in methanol (20 ml) and 9-hydroxyfluorene-9-carboxylic acid (0.44 g,
Bis(9-hydroxyfluorene-9-carboxylato-κ2O,O′)tripyridinecadmium(II)
✍ Scribed by Gao, Shan ;Huo, Li-Hua ;Lu, Zhen-Zhong ;Zhao, Hui
- Publisher
- International Union of Crystallography
- Year
- 2004
- Tongue
- English
- Weight
- 321 KB
- Volume
- 60
- Category
- Article
- ISSN
- 1600-5368
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📜 SIMILAR VOLUMES
Single-crystal X-ray study T = 298 K Mean '(C±C) = 0.003 A Ê R factor = 0.028 wR factor = 0.067 Data-to-parameter ratio = 12.5 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.
The title compound, [Co(C 10 H 7 NO 3 ) 2 ]Á3H 2 O, contains sixcoordinate Co II with a mer-octahedral arrangement. The central Co atom is coordinated by the hydroxyl O atom, the quinoline N atom and a carboxylate O atom of each of the two tridentate ligands.
Single-crystal X-ray study T = 295 K Mean '(C±C) = 0.005 A Ê Disorder in solvent or counterion R factor = 0.034 wR factor = 0.086 Data-to-parameter ratio = 15.2 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.