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Biocatalytic synthesis of (S)-2-tridecanyl acetate and (S)-2-pentadecanyl acetate, aggregation pheromone components ofDrosophila mulleriandD. busckii, by enantioselective hydrolysis with lipase

✍ Scribed by Makoto Kamezawa; Hojun Tachibana; Takehiko Ohtani; Yoshinobu Naoshima

Publisher: Springer
Year: 1994
Tongue: English
Weight: 289 KB
Volume: 20
Category: Article
ISSN: 0098-0331
DOI: 10.1007/bf02059742

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## Abstract The enantioselective synthesis of (__S__)‐(+)‐2‐tridecanol acetate [(__S__)‐6] (ee = 93.5%), an aggregation pheromone of __Drosophila mulleri__, is described. Key steps are the α‐alkylation of the propiophenone SAMP‐hydrazone (__S__)‐2 (de ≥ 96%) and the Baeyer‐Villiger reaction of the